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1 article(s) from Beer, Paul D

A ferrocene redox-active triazolium macrocycle that binds and senses chloride

Nicholas G. White and
Paul D. Beer

Beilstein J. Org. Chem. 2012, 8, 246–252, doi:10.3762/bjoc.8.25

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Scheme 1: Synthesis of bis(triazole) macrocycle 3 and tetra(triazole) macrocycle 4. Conditions and reagents: ...

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Scheme 2: Synthesis of bis(triazolium) macrocycle, 5. Conditions and reagents: (i) (a) (Me₃O)(BF₄), CH₂Cl₂, (...

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Figure 1: Solid-state structure of 3 (left) and 4 (right). Hydrogen atoms omitted for clarity, ellipsoids are...

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Figure 2: ¹H NMR spectra of 5·2PF₆ after the addition of 0, 1.0, 2.0 and 5.0 equiv of TBA·Cl (500 MHz, 293 K,...

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Figure 3: Titration data (solid points) and fitted binding isotherms (curves) monitoring the triazolium proto...

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Figure 4: CV of 5·2PF₆ upon the addition of TBA·Cl (electrolyte: 0.1 M TBA·PF₆/CH₃CN, [5·2PF₆] = 0.50 mM, 293...

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Published 13 Feb 2012

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